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Convenient Synthesis of N,N′-Bis-protected-3,3′-diiodo-2,2′-biindoles.

✍ Scribed by Sudipta Roy; Gordon W. Gribble

Publisher
John Wiley and Sons
Year
2007
Weight
24 KB
Volume
38
Category
Article
ISSN
0931-7597

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1251 Amiodarone was prepared by iodination of 1 2SI 251 amiodarone was obtained 2-n butyl 4-hydroxy 3-benzoyl benzofuran with Na in alkaline medium. By amination with N8N-diethyl 2-amino 1 -chloroethane, with 30 % yield and a specific activity of about 1 Ci/mmOl.