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Convenient Catalytic Synthesis and Assignment of the Absolute Configuration of Enantiomerically Pure Dihydronaphthalenes and Their Corresponding Epoxides

✍ Scribed by Torsten Linker; Frank Rebien; Gábor Tóth; András Simon; Jürgen Kraus; Gerhard Bringmann

Publisher
John Wiley and Sons
Year
1998
Tongue
English
Weight
195 KB
Volume
4
Category
Article
ISSN
0947-6539

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is therefore generated in situ from trichloroacetohydroximoyl chloride (4)['l. While oxepin reacts directly with ( 1 ) to give (3), reaction of ( 1 ) with 1,3-cyclohexadiene gives cycloadduct ( 5 ) as intermediate. This thermally labile compound rearranges even at room temperature, and more rapidly