Controlled thermal degradation for the identification and quantification of amine N-oxides in urine
✍ Scribed by Boel Lindegård; Lennart Mathiasson; Jan Åke Jönsson; Bengt Åkesson
- Book ID
- 108337146
- Publisher
- Elsevier Science
- Year
- 1990
- Tongue
- English
- Weight
- 765 KB
- Volume
- 514
- Category
- Article
- ISSN
- 1873-3778
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## Abstract Two simple and rapid LC/MS methods with direct injection analysis were developed and validated for the quantification and identification of hydrocortisone in equine urine using the same sample preparation but different mass spectrometric systems: ion trap mass spectrometry (IT‐MS) and t
We wish to report direct evidence for a homolytic scission-recombination mechanism in the thermal eMeisenheimer" rearrangement' of the title compound, I, to the hydroxylamine, II (equation I). This mechanism W&B apparently first proposed by Schgllkopf,3 who adduced threefold