Construction of the Tetracyclic Skeleton of Leucothol A. 1,2,4a,5,6,7,8,9,10,10a,11,11a-Dodecahydro-11-hydroxy-11-methyl-7-phenylthiomethyl-5aH-5a,8-methanocyclohepta[b]naphthalen-10-one
✍ Scribed by Kraus, G. A. ;Su, Q. ;Young Jnr, V. G.
- Book ID
- 114511780
- Publisher
- International Union of Crystallography
- Year
- 1995
- Tongue
- English
- Weight
- 285 KB
- Volume
- 51
- Category
- Article
- ISSN
- 0108-2701
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📜 SIMILAR VOLUMES
Single-crystal X-ray study T = 183 K Mean '(C±C) = 0.003 A Ê R factor = 0.035 wR factor = 0.082 Data-to-parameter ratio = 12.6 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
The title compound, C 25 H 20 ClN 3 O 2 ÁC 3 H 7 NO, was synthesized by the reaction of 4-chlorobenzaldehyde, 2-(5,5-dimethyl-3oxocyclohex-1-enylamino)benzoic acid and malononitrile in ethylene glycol under microwave irradiation. The dihydropyridine and pyrimidine rings both adopt boat conformations