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Conjugated Microporous Poly(aryleneethynylene) Networks

✍ Scribed by Jia-Xing Jiang; Fabing Su; Abbie Trewin; Colin D. Wood; Neil L. Campbell; Hongjun Niu; Calum Dickinson; Alexey Y. Ganin; Matthew J. Rosseinsky; Yaroslav Z. Khimyak; Andrew I. Cooper

Publisher
John Wiley and Sons
Year
2008
Tongue
English
Weight
157 KB
Volume
120
Category
Article
ISSN
0044-8249

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Conjugated Microporous Poly(aryleneethyn
Conjugated Microporous Poly(aryleneethynylene) Networks
✍ Jia-Xing Jiang; Fabing Su; Abbie Trewin; Colin D. Wood; Neil L. Campbell; Hongju 📂 Article 📅 2008 🏛 John Wiley and Sons 🌐 English ⚖ 157 KB

The ratio of intensities of acetylene to aromatic peaks was calculated using variable-contact-time 1 H-13 C CP/MAS NMR spectra with the following results: CMP-1 0.27 (expected value 0.40); CMP-2 0.18 (expected value 0.25); CMP-3 0.10 (expected value 0.18).

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π-Conjugated microporous networks have been prepared from the tetraarylated diketopyrrolo[3,4-__c__]pyrrole unit as a tetrafunctional building block. The reactions are carried out using microwave-assisted Yamamoto or Sonogashira cross-coupling. Red insoluble powders are obtained, showing intense flu