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Conformational Study of Solid Polypeptides by 1 H Combined Rotation and Multiple Pulse Spectroscopy NMR

โœ Scribed by Shoji, Akira; Kimura, Hideaki; Ozaki, Takuo; Sugisawa, Hisashi; Deguchi, Kenzo


Book ID
118195998
Publisher
American Chemical Society
Year
1996
Tongue
English
Weight
129 KB
Volume
118
Category
Article
ISSN
0002-7863

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Technical details are given for the successful operation of CRAMPS techniques to obtain high-resolution proton NMR spectra of solids. Matters addressed include probe construction, tuning procedures, optimization of pulses, spectral calibration and referencing. In practice, the MREV-8 sequence is pre