𝔖 Bobbio Scriptorium
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A practical guide to combined rotation and multiple-pulse NMR spectroscopy of solids

✍ Scribed by Peter Jackson; Robin K. Harris

Publisher
John Wiley and Sons
Year
1988
Tongue
English
Weight
836 KB
Volume
26
Category
Article
ISSN
0749-1581

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✦ Synopsis

Technical details are given for the successful operation of CRAMPS techniques to obtain high-resolution proton NMR spectra of solids. Matters addressed include probe construction, tuning procedures, optimization of pulses, spectral calibration and referencing. In practice, the MREV-8 sequence is preferred to BR-24. It is suggested that CRAMPS operation deserves more widespread application.

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Three multiple-pulse spin-echo experiments that have been used to enhance the sensitivity of broad powder patterns obtained from NMR spectra of spin-1/2 and half-integer quadrupolar nuclei in polycrystalline solids are examined. Specifically, the Carr-Purcell Meiboom-Gill (CPMG), the Mansfield-Waugh