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Conformational properties of 4,4,7,7-tetramethyl-2-hetero-1,3-dioxepanes

✍ Scribed by B. A. Arbuzov; V. V. Klochkov; P. P. Chernov; H. I. Borisenko; L. K. Yuldasheva

Book ID
112448058
Publisher
Springer
Year
1987
Tongue
English
Weight
378 KB
Volume
36
Category
Article
ISSN
1573-9171

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A dynamic nuclear magnetic resonance spe
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## Abstract The 251 MHz ^1^H and the natural abundance 63.1 MHz ^13^C NMR spectra of 1,3‐dioxepane (1) and 4,4,7,7‐tetramethyl‐1,3‐dioxepane (2) have been investigated over the temperature range of 5 to βˆ’180 Β°C. While the spectra of 1 show no dynamic NMR effect, compound 2 exists in solution as a 1