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Conformational Preferences of Natural and C3-Modified Epothilones in Aqueous Solution

✍ Scribed by Erdélyi, Máté; Pfeiffer, Bernhard; Hauenstein, Kurt; Fohrer, Jörg; Gertsch, Jürg; Altmann, Karl-Heinz; Carlomagno, Teresa

Book ID
118054364
Publisher
American Chemical Society
Year
2008
Tongue
English
Weight
537 KB
Volume
51
Category
Article
ISSN
0022-2623

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Conformational study of phosphothreonine
Conformational study of phosphothreonine in aqueous solution. H and 13C NMR results
✍ L. Pogliani; D. Ziessow 📂 Article 📅 1978 🏛 John Wiley and Sons 🌐 English ⚖ 250 KB 👁 1 views

## Abstract The 270 MHz ^1^H and 22.6 MHz ^13^C NMR spectra of DL‐phosphothreonine in D~2~O have been measured and analysed as a function of pD. The __trans__‐__trans__ conformation of the fragment H‐αC‐αC‐βOP predominates at all pD values. The C‐β—O __gauche__ contribution is notably larger fo