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Conformational analysis. X. Determination of intramolecular hydrogen bonding by hydroxyl proton magnetic resonance

โœ Scribed by Ouellette, Robert J.; Liptak, Kathleen; Booth, Gary E.

Book ID
127231554
Publisher
American Chemical Society
Year
1967
Tongue
English
Weight
545 KB
Volume
32
Category
Article
ISSN
0022-3263

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The proton magnetic resonance spectrum of thyrotropin releasing factor (TRF) in solution in deuterium oxide and deuterated dimethylsulfoxide (DMSO-d6) has been analyzed. Two forms differing in cis-trans isomerism about the His-Pro peptide bond are observed. From the temperature dependence of chemica