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Conformation of hindered piperidines: Spectroscopic evidence for contribution of boat conformations

✍ Scribed by A. Thangamani; J. Jayabharathi; A. Manimekalai

Book ID
107584663
Publisher
Indian Academy of Sciences,Royal Society of Chemistry
Year
2010
Tongue
English
Weight
267 KB
Volume
122
Category
Article
ISSN
0253-4134

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For a review of recent activity, see [l]. ## For other ref., see [3]. For a review on methods to determine thermodynamic parameters by dynamic NMR, see [5].

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## Abstract The PMR spectrum of 2‐bromo‐4,6‐dinitrophenyl 2′‐naphthyl ether (**1**) is consistent with the preferential adoption of a twist conformation (**1a**) in which the 6‐nitro group and the 1′‐hydrogen are located __endo__ to the ether link. This preference is explained by the formation of a