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Confirmation of the structure of a glucono-1,4-lactone derivative obtained from silylation of glucono-1,5-lactone

✍ Scribed by Paul V. Murphy; Ciaran McDonnell; Ludger Hämig; Duncan E. Paterson; Richard J.K. Taylor

Book ID
104359552
Publisher
Elsevier Science
Year
2003
Tongue
English
Weight
299 KB
Volume
14
Category
Article
ISSN
0957-4166

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✍ Diane R. Wolk; Andrea Vasella; Fritz Schweikart; Martin G. Peter 📂 Article 📅 1992 🏛 John Wiley and Sons 🌐 German ⚖ 707 KB

The carbohydrate-derived lactone phenylsemicarbazones 3 and 4 were prepared from 5 and 8 (Scheme). Treatment with 4-phenylsemicarbazide gave 6 and 7 (77:23) and 9 and 10 (76:24), respectively. Oxidation of 6 and 9 by Cr0,-pyridine to 11 and 13, followed by deprotection, yielded 3 and 4. The structur