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Concise total synthesis of 9-methoxystrobilurin A

✍ Scribed by Hiromi Uchiro; Koh Nagasawa; Yasuyuki Aiba; Susumu Kobayashi

Publisher
Elsevier Science
Year
2000
Tongue
French
Weight
156 KB
Volume
41
Category
Article
ISSN
0040-4039

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✦ Synopsis

Total synthesis of a potent antifungal and cytostatic 9-methoxystrobilurin A was achieved by developing a concise and general route to Ξ²-methoxy acrylate.

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potent antifungal and cytostatic 9-methoxystrobilurin K was achieved by developing a convergent and versatile synthetic route.

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## Abstract For Abstract see ChemInform Abstract in Full Text.

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## Abstract A practical synthesis of the necine base (+)‐heliotridine (**1**) is reported here. The present total synthesis is based on the highly selective 1,3‐dipolar cycloaddition of (__S__)‐3‐__tert__‐butoxypyrroline __N__‐oxide (**2**) to the commercially available ethyl 4‐bromocrotonate, foll