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Computational study of the Sonogashira cross-coupling reaction in the gas phase and in dichloromethane solution

✍ Scribed by Lauri Sikk, Jaana Tammiku-Taul, Peeter Burk, András Kotschy

Book ID
113053386
Publisher
Springer-Verlag
Year
2011
Tongue
English
Weight
496 KB
Volume
18
Category
Article
ISSN
1610-2940

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✍ Bernard Deschamps; Xavier Le Goff; Louis Ricard; Pascal Le Floch 📂 Article 📅 2007 🏛 John Wiley and Sons 🌐 English ⚖ 359 KB

## Abstract The 1‐methoxy‐2‐(supermesitylphosphanylidenemethyl)‐benzene ligand (**1**) was prepared by reacting the phospha‐Wittig reagent [Mes\*PPMe~3~] with o‐methoxybenzaldehyde. Reaction of 1 with one equivalent of the [Pd(allyl)Cl]~2~ dimer in the presence of Ag(OTf) affords a neutral complex