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Complete proton and carbon-13 NMR assignment of the alkaloid gephyrotoxin through the use of homonuclear Hartmann-Hahn and two-dimensional spectroscopy

โœ Scribed by Edwards, Michael W.; Bax, Ad.


Book ID
126150036
Publisher
American Chemical Society
Year
1986
Tongue
English
Weight
770 KB
Volume
108
Category
Article
ISSN
0002-7863

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## Abstract The identification and complete ^13^C and ^1^H assignment of a sample of oligomycin A is described. ^13^C multiplicities were determined by the INEPT method; assignments were made by comparison of heteronuclear ^13^Cโ€^1^H chemical shift correlation, homonuclear COSY and homonuclear rela