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Concerted use of two-dimensional NMR techniques in the ab initio assignment of complex spectra: Complete proton and carbon-13 assignment of oligomycin A

✍ Scribed by Gareth A. Morris; Michelle S. Richards

Publisher: John Wiley and Sons
Year: 1985
Tongue: English
Weight: 741 KB
Volume: 23
Category: Article
ISSN: 0749-1581
DOI: 10.1002/mrc.1260230815

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✦ Synopsis

Abstract

The identification and complete ^13^C and ^1^H assignment of a sample of oligomycin A is described. ^13^C multiplicities were determined by the INEPT method; assignments were made by comparison of heteronuclear ^13^C‐^1^H chemical shift correlation, homonuclear COSY and homonuclear relayed coherence transfer two‐dimensional NMR spectra.

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