𝔖 Bobbio Scriptorium
✦   LIBER   ✦

Complete assignments of the 1H and 13C NMR spectra of five rearranged abietane diterpenoids

✍ Scribed by Benjamín Rodríguez


Publisher
John Wiley and Sons
Year
2002
Tongue
English
Weight
86 KB
Volume
40
Category
Article
ISSN
0749-1581

No coin nor oath required. For personal study only.

✦ Synopsis


Abstract

An NMR study of five highly functionalized and rearranged abietane diterpenoids is described. In addition to 1D NMR methods, including 1D NOESY spectra, 2D shift‐correlated experiments [^1^H, ^13^C‐gHSQC‐^1^J (C,H) and ^1^H, ^13^C‐gHMBC‐^n^J (C,H) (n = 2 and 3)] were used for the complete and unambiguous ^1^H and ^13^C chemical shift assignments of these substances. Copyright © 2002 John Wiley & Sons, Ltd.


📜 SIMILAR VOLUMES


1H and 13C NMR spectral assignments of s
✍ Benjamín Rodríguez 📂 Article 📅 2003 🏛 John Wiley and Sons 🌐 English ⚖ 112 KB 👁 1 views

## Abstract An NMR study of 11 naturally occurring abietane diterpenoids is described. In addition to one‐dimensional NMR methods, including DPFGSE 1D‐NOE spectra, two‐dimensional shift‐correlated experiments [^1^H,^1^H COSY, ^1^H,^13^C‐gHSQC ^1^__J__(C,H) and ^1^H,^13^C‐gHMBC ^__n__^__J__(C,H) (__

Complete assignments of the 1H and 13C N
✍ Benjamín Rodríguez 📂 Article 📅 2001 🏛 John Wiley and Sons 🌐 English ⚖ 172 KB

## Abstract An NMR study of six highly functionalized neoclerodane diterpenes belonging to both A/B __cis__ and __trans__ series is described. In addition to 1D NMR methods, 2D shift‐correlated experiments [^1^H,^1^H‐COSY, ^1^H,^1^H‐TOCSY, ^1^H,^13^C‐gHSQC‐^1^__J__(C,H), ^1^H,^13^C‐gHMBC‐^__n__^__J

Complete assignment of 1H and 13C NMR sp
✍ Minoru Takekawa; Junji Aoki; Satoshi Iwashima; Toyotoshi Ueda 📂 Article 📅 1994 🏛 John Wiley and Sons 🌐 English ⚖ 457 KB

## Abstract ^1^H and ^13^C NMR studies were carried out on benzanthrone and 3‐, 4‐, 6‐, 8‐, 9‐, 10‐ and 11‐chlorobenzanthrone. Complete assignments of proton and carbon resonances were made with the aid of HH‐COSY, NOESY, CH‐COSY and HMBC techniques. Substitution effects of a chlorine atom are not

Complete 1H and 13C NMR assignments of c
✍ Gianfranco Fontana; Giuseppe Savona; Benjamín Rodríguez 📂 Article 📅 2006 🏛 John Wiley and Sons 🌐 English ⚖ 150 KB 👁 1 views

## Abstract Unambiguous and complete assignments of ^1^H and ^13^C NMR chemical shifts for five clerodane diterpenes, four of them isolated from __Salvia splendens__ (salviarin, splendidin and splenolides A and B) and one obtained by acetylation of splenolide A, are presented. The assignments are b