Complete assignments of the 1H and 13C NMR spectra of 9,10-didehydro retinoic acids
✍ Scribed by J. Thibonnet; A. Duchêne; J.-L. Parrain; M. Abarbri
- Publisher
- John Wiley and Sons
- Year
- 2006
- Tongue
- English
- Weight
- 84 KB
- Volume
- 44
- Category
- Article
- ISSN
- 0749-1581
- DOI
- 10.1002/mrc.1800
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✦ Synopsis
Abstract
A new class of retinoic acids was synthesized containing a 9,10‐rigid bond. ^1^H and ^13^C NMR spectra were assigned for eight new compounds (all‐E, 13__Z__) containing a carboxylic acid or tertiobutylester polar end group. Assignments were based on the combination of one‐ and two‐ dimensional experiments (APT, COSY, HMBC). Copyright © 2006 John Wiley & Sons, Ltd.
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