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Complete assignment of 19F, 1H and 13C NMR spectra of monomers and precursors towards bridge trifluoromethylated poly(p-phenylenevinylene)

✍ Scribed by Alex J. Roche

Publisher
John Wiley and Sons
Year
2004
Tongue
English
Weight
115 KB
Volume
42
Category
Article
ISSN
0749-1581

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✦ Synopsis

Abstract

The complete assignment of ^19^F, ^1^H and ^13^C NMR spectra of 11 trifluoromethylated and four bistrifluoromethylated monomers for bridge trifluoromethylated poly(p‐phenylenevinylene) is described. The combination of one‐dimensional ^19^F, ^1^H and ^13^C spectra, long‐range fluorine couplings and the two‐dimensional techniques of direct and long‐range HETCOR (J = 140 and 8 Hz) permitted full resonance assignment. Copyright © 2004 John Wiley & Sons, Ltd.

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