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Complete assignment of 1H and 13C NMR spectra of a set of sulphinyl and sulphonyl monomers toward poly(p-phenylenevinylene) precursors

✍ Scribed by Albert J. J. M. van Breemen; Peter J. Adriaensens; Anna C. J. Issaris; Margreet M. de Kok; Dirk J. M. Vanderzande; Jan M. J. V. Gelan

Publisher: John Wiley and Sons
Year: 2000
Tongue: English
Weight: 76 KB
Volume: 38
Category: Article
ISSN: 0749-1581
DOI: 10.1002/(sici)1097-458x(200002)38:2<129::aid-mrc602>3.0.co;2-k

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✦ Synopsis

The complete assignment of the 1 H and 13 C NMR spectra of sulphinyl and sulphonyl monomers toward poly(p-phenylenevinylene) precursors is presented. For all compounds the same protocol could be used. Resonance assignments were achieved by the use of one-and two dimensional NMR techniques such as 1 H, 13 C APT and 2D HETCOR (J D 8 Hz, J D 140 Hz), INADEQUATE and COSY.

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