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Complete 1H and 13C NMR spectral assignment of pentacyclo [6.4.0.02,6.05,9.04,12]dodecane derivatives and structure elucidation of pentacyclo [6.4.0.02,6.03,11.05,9]dodecane

✍ Scribed by F. J. C. Martins; G. H. Coetzee; L. Fourie; H. J. Venter; A. M. Viljoen; P. L. Wessels

Publisher
John Wiley and Sons
Year
1993
Tongue
English
Weight
605 KB
Volume
31
Category
Article
ISSN
0749-1581

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✦ Synopsis

Abstract

Treatment of pentacyclo[6.4.0.0^2,6^.0^5,9^.0^4,12^]dodecane‐2‐ol with concentrated sulphuric acid produced the rearranged hydrocarbon pentacyclo[6.4.0.0^2,6^.0^3,11^.0^5,9^]dodecane as the main product. High‐field ^1^H and ^13^C NMR techniques were used in the structure elucidation and assignment of the different NMR resonances of these two and related compounds.

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