𝔖 Bobbio Scriptorium
✦   LIBER   ✦

Complete 1H and 13C NMR assignments of two new trans-clerodane diterpenoids from Otostegia limbata

✍ Scribed by Umar Farooq; Afsar Khan; Viqar Uddin Ahmad; Azhar-Ul-Haq; Saleha Suleman Khan; Robina Farooq; Arshid Pervez; Mohammad Mahroof Shah


Publisher
John Wiley and Sons
Year
2007
Tongue
English
Weight
132 KB
Volume
45
Category
Article
ISSN
0749-1581

No coin nor oath required. For personal study only.

✦ Synopsis


Abstract

Two new tricyclic trans‐clerodane diterpenoids trivially named as ballotenic acid A (1) and ballodiolic acid A (2) have been isolated from ethyl acetate fraction of Otostegia limbata. The structure assignments are based on ^1^H and ^13^C NMR spectra, 2D NMR (HMQC, HMBC, COSY, NOESY and NOE) techniques and comparison with the literature data. Copyright © 2007 John Wiley & Sons, Ltd.


📜 SIMILAR VOLUMES


Complete 1H and 13C NMR assignments of c
✍ Gianfranco Fontana; Giuseppe Savona; Benjamín Rodríguez 📂 Article 📅 2006 🏛 John Wiley and Sons 🌐 English ⚖ 150 KB 👁 1 views

## Abstract Unambiguous and complete assignments of ^1^H and ^13^C NMR chemical shifts for five clerodane diterpenes, four of them isolated from __Salvia splendens__ (salviarin, splendidin and splenolides A and B) and one obtained by acetylation of splenolide A, are presented. The assignments are b

Complete 1H and 13C NMR assignment of tr
✍ Irena Škorić; Željko Marinić; Krešimir Molčanov; Biserka Kojić-Prodić; Marija Ši 📂 Article 📅 2007 🏛 John Wiley and Sons 🌐 English ⚖ 188 KB

## Abstract ^1^H and ^13^C NMR spectra of __trans, trans__‐2,3‐divinylfuran derivatives (1–4) in CDCl~3~ were fully assigned using one‐ and two‐dimensional NMR techniques. The ^1^H NMR resonances of ethylenic protons in position 2 with regard to the corresponding protons in position 3 of the furan

Complete 1H and 13C NMR assignments of f
✍ Jiaquan Feng; Weimin Zhao 📂 Article 📅 2009 🏛 John Wiley and Sons 🌐 English ⚖ 122 KB

## Abstract Four new oligosaccharides (1–4), one new pregnane glycoside (5), and one new cardiac glycoside (6) were isolated from the roots of __Periploca forrestii__ Schltr. (Asclepiadaceae), a traditional Chinese medicine used for the treatment of rheumatoid arthritis and wounds. Their structures

Complete assignments of the 1H and 13C N
✍ Benjamín Rodríguez 📂 Article 📅 2002 🏛 John Wiley and Sons 🌐 English ⚖ 86 KB 👁 1 views

## Abstract An NMR study of five highly functionalized and rearranged abietane diterpenoids is described. In addition to 1D NMR methods, including 1D NOESY spectra, 2D shift‐correlated experiments [^1^H, ^13^C‐gHSQC‐^1^__J__ (C,H) and ^1^H, ^13^C‐gHMBC‐^__n__^__J__ (C,H) (__n__ = 2 and 3)] were use