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Complete 1H and 13C assignments of (21R) and (21S) diastereomers of argatroban

โœ Scribed by Diego Colombo; Patrizia Ferraboschi; Paride Grisenti; Laura Legnani

Publisher
John Wiley and Sons
Year
2007
Tongue
English
Weight
138 KB
Volume
46
Category
Article
ISSN
0749-1581

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โœฆ Synopsis

Abstract

The complete ^1^H and ^13^C NMR assignments are reported for the antithrombotic (21__R__)โ€ and (21__S__)โ€argatroban by 1D and 2D NMR experiments (HSQC, HMBC, NOESY and ^1^H๏ฃฟ^1^H COSY). Some wellโ€resolved signals could be used for an accurate measurement of the diastereomeric composition of argatroban. Copyright ยฉ 2008 John Wiley & Sons, Ltd.

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