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Comparison of structure-thermal property relationships for barium bis(1,1,1,5,5,5-hexafluoro-2,4-pentanedionate) polyether complexes

✍ Scribed by Halina D. Inerowicz; Thekkekalathil M. Chandrasekhar; Gordon Atkinson; Robert L. White

Publisher: Elsevier Science
Year: 1994
Tongue: English
Weight: 810 KB
Volume: 289
Category: Article
ISSN: 0003-2670
DOI: 10.1016/0003-2670(94)80109-6

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✦ Synopsis

The thermal properties of Ba(hfa),, Ba(hfa),(tetraglyme), Ba(hfa)l(18-crownd), and Ba(hfa)&diaza-1%crown-61 are investigated by comparing the results of thermogravimetric analysis (TGA) for these materials. All TGA measurements were made in helium at atmospheric pressure. Infrared, MS, NMR, and x-ray crystallographic measurements are compared for each of the complexes and correlations are made between the structure-specific information derived from these analyses and the thermal properties of the barium complexes.

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