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Comparison of electrochemical and enzymic oxidation of 1,3-dimethyluric acid

โœ Scribed by Rajendra N. Goyal; Naveen K. Singhal


Book ID
108431240
Publisher
Elsevier Science
Year
1998
Tongue
English
Weight
430 KB
Volume
44
Category
Article
ISSN
1567-5394

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A synthetic procedure for l13-di(trideuteromethyl)uric acid is described. Deuterium labeling of the N-1 and N-3 positions w a s achieved by methylation of 4-amino-5carbethoxyuracil with di( trideuteromethy1)-sulfate followed by cyclization of the dimethylated intermediate by heating. The synthesis r