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Comparison of different 2D NMR techniques for 13C, 31P correlation

✍ Scribed by Peter Bast; Stefan Berger; Harald Günther

Publisher
John Wiley and Sons
Year
1992
Tongue
English
Weight
496 KB
Volume
30
Category
Article
ISSN
0749-1581

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✦ Synopsis

Abstract

Three different experimental techniques are compared to find the most efficient protocol for 2D ^13^C, ^31^P correlation spectroscopy. It is shown that the best signal‐to‐noise ratio is given by the polarization transfer experiment for ^31^P detection and by the HMQC experiment for ^13^C detection. Applications of these techniques for ^13^C,^31^P correlation of β‐nicotinamide adenine dinucleotide (NAD^+^) and a mixture of three different mononucleotides are described.

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