Comparison between cellulose and amylose tris(3,5-dimethylphenylcarbamate) chiral stationary phases for enantiomeric separation of 17 amidotetralins
✍ Scribed by Dr. Dirk T. Witte; Frank J. Bruggeman; Jan Piet Franke; Swier Copinga; Johanna M. Jansen; Rokus A. De Zeeuw
- Publisher
- John Wiley and Sons
- Year
- 1993
- Tongue
- English
- Weight
- 704 KB
- Volume
- 5
- Category
- Article
- ISSN
- 0899-0042
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## Abstract A novel cellulose tris(__N__‐3,5‐dimethylphenylcarbamate) (CDMPC) chiral stationary phase (CSP) was prepared by coating CDMPC on TiO~2~/SiO~2~, which was prepared by coating titania nanoparticles on silica through a self‐assemble technique. At first, 2‐hydroxyl‐phenyl acetonitrile and _
Cellulose-tris(3,5-dimethylphenylcarbamate) was prepared after a reported method and was coated onto an aminopropylated mesopore spherical silica gel. The final product was used as a chiral stationary phase of high performance liquid chromatography for the enantioseparation of a series of glycerin s