For reliable confirmation of peptide structures, nozzle-skimmer collisionally induced dissociation was found in many cases to be insufficient, and partial acid hydrolysis was employed as a complementary technique. The utility of combining these fragmentation methods is demonstrated in two examples w
Combined Partial Acid Hydrolysis and Electrospray Ionization-Mass Spectrometry for the Structural Determination of Oligosaccharides
✍ Scribed by Cancilla, Mark T.; Gaucher, Sara P.; Desaire, Heather; Leary, Julie A.
- Book ID
- 120212971
- Publisher
- American Chemical Society
- Year
- 2000
- Tongue
- English
- Weight
- 105 KB
- Volume
- 72
- Category
- Article
- ISSN
- 0003-2700
No coin nor oath required. For personal study only.
📜 SIMILAR VOLUMES
## Abstract Derivatization procedures using 1‐phenyl‐3‐methyl‐5‐pyrazolone (PMP) and 2‐aminonaphthalene trisulfone (ANTS) were selected among a number of well known methods for labelling carbohydrates. PMP derivatives were selected owing to our laboratory's previous high‐performance liquid chromato
Structural analyses of oligosaccharide-malononitrile derivatives were conducted by matrix-assisted laser desorption/ionization post-source decay (MALDI-PSD) analysis in positive ion mode, and by electrospray ionization collision-induced dissociation (ESI-CID) analysis in negative ion mode. The malon
Flucofuron and sulcofuron, both examples of mitins, have been employed as the active ingredients in mothproofing formulations for the protection of textile fabrics by the dyeing industry. Monitoring of their presence in components of the river ecosystem is a regulatory requirement so that sensitive
The use of electrospray Ionization (ESI) tandem mass spectrometry (MS/MS) for the structural determination of the lipid A components of the psychrophilic bacterium Pseudoalteromonas haloplanktis TAC 125 is reported. The lipid A contains the classical bisphosphorylated beta-(1' --> 6)-linked D-glucos