A cold decomposition procedure for the spectrophotometric determination of manganese in rocks, ores and minerals is described. Samples are allowed to react with hydrofluoric acid and aqua regia at room temperature for 24 h. Fluoride'ions in the solution are complexed with boric acid and manganese is
Cold decomposition procedure for the spectrophotometric determination of titanium in ores and minerals
β Scribed by G.S. Reddi; C.R.M. Rao; T.A.S. Rao; H.S. Muralidhar
- Publisher
- Elsevier Science
- Year
- 1991
- Tongue
- English
- Weight
- 138 KB
- Volume
- 251
- Category
- Article
- ISSN
- 0003-2670
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β¦ Synopsis
A cold decomposition procedure for the spetrophotometric determination of titanium in ores and minerals is described. Samples are allowed to react with hydrofluoric acid and aqua regia at room temperature overnight. Fluoride ions in the solution are complexed with boric acid and the titanium is determined using Tiron. As fluoride ions do not have to be removed by heating, the method is rapid and avoids the use of platinum ware.
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An acid decomposltlon procedure at room temperature for the spectrophotometnc determmatlon of slhca m rocks and minerals 1s described The sample solution IS prepared by treatment with hydrotluorlc acid and aqua regla at room temperature Unreacted fluoride ions are complexed Hrlth bone acid and the s
A kinetic method for the simultaneous determination of iron, titanium and vanadium is proposed based on their inductive effects on the chromium(VI)-iodide-starch reaction in weakly acidic medium. The reaction was monitored with the stopped-flow spectrophotometric technique. The calibration graphs ar