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Cluster-to-Metal Magnetic Coupling: Synthesis and Characterization of 25-Electron [Re 6- n Os n Se 8 (CN) 6 ] (5- n )- ( n = 1, 2) Clusters and {Re 6- n Os n Se 8 [CNCu(Me 6 tren)] 6 } 9+ ( n = 0, 1, 2) Assemblies

✍ Scribed by Tulsky, Eric G.; Crawford, Nathan R. M.; Baudron, Stéphane A.; Batail, Patrick; Long, Jeffrey R.

Book ID: 126413710
Publisher: American Chemical Society
Year: 2003
Tongue: English
Weight: 232 KB
Volume: 125
Category: Article
ISSN: 0002-7863
DOI: 10.1021/ja037444q

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R1 ‫؍‬ 0.0387, wR2 ‫؍‬ 0.0624), (Pr 4 N) 2 Mn(H 2 O) 4 [Re 6 S 8 (CN) 6 ] (space group: I4/m, a ‫؍‬ 13.255(2) A s , c ‫؍‬ 14.432(3) A s , V ‫؍‬ 2535.6(8) A s 3 , R1 ‫؍‬ 0.0369, wR2 ‫؍‬ 0.0960) and (Pr 4 N) 2 Ni (H 2 O) 4 [Re 6 S 8 (CN) 6 ] (space group: I4/m, a ‫؍‬ 13.247(4) A s , c ‫؍‬ 14.246(6) A