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Cluster compounds [Ca(DMF)6][Mo6Cl14] and [{Ca(OPPh3)4}{Mo6Cl14}]∞: Synthesis, crystal structure, and properties

✍ Scribed by Zh. S. Kozhomuratova; Yu. V. Mironov; M. A. Shestopalov; Ya. M. Gaifulin; N. V. Kurat’eva; E. M. Uskov; V. E. Fedorov

Book ID
111457970
Publisher
SP MAIK Nauka/Interperiodica
Year
2007
Tongue
English
Weight
298 KB
Volume
33
Category
Article
ISSN
1070-3284

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Synthesis, Structure, and Decomposition
Synthesis, Structure, and Decomposition of (NH4)2[Mo6Cl14] · H2O
✍ Andreas Nägele; Katharina Gibson; Abdessadek Lachgar; H.-Jürgen Meyer 📂 Article 📅 1999 🏛 John Wiley and Sons 🌐 German ⚖ 106 KB 👁 1 views

NH 4 ) 2 [Mo 6 Cl 14 ] ´H2 O (1) was prepared from reactions of MoCl 2 in ethanol with aqueous NH 4 Cl solution. It crystallizes in the monoclinic space group I2/a (no. 15), Z = 4 with a = 912.3(1), b = 1491.2(2), c = 1724.8(2) pm, b = 92.25(1)°; R1 = 0.023 (based on F values) and wR2 = 0.059 (based