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Clarification of the mechanism of rearrangement of enol silyl ether epoxides

✍ Scribed by G.M. Rubottom; J.M. Gruber; R.K. Boeckman Jr.; M. Ramaiah; J.B. Medwid

Publisher
Elsevier Science
Year
1978
Tongue
French
Weight
215 KB
Volume
19
Category
Article
ISSN
0040-4039

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Phenylthiomethylstannylation of silyl en
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Silyl enol ethers (2) react with trihutyl [(phenylthio) chloromethyl] stannane (1) in the presence of Zinc bromide to give B-phenylthiomethylstannyl ketones (3) in good yields. Silyl dienol ethers (4) mainly give products (5) due to y-attack, under these conditions. S-Stannyl Carbonyl compounds have