Chromatography of food preservatives on polyamide layers and columns
β Scribed by Kinzo Nagasawa; Hisae Yoshidome; Ryuzo Takeshita
- Publisher
- Elsevier Science
- Year
- 1969
- Tongue
- English
- Weight
- 580 KB
- Volume
- 43
- Category
- Article
- ISSN
- 1873-3778
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β¦ Synopsis
The separation of eight kinds of food preservative by one-and two-dimensional chromatography on polyamide layers was investigated.
A comparison was made between the detection limits on polyamide and silica gel layers, and the superiority of the polyamide thin layers was confirmed.
The separation of the food preservatives on a polyamide column with two types of elution system was established. The recovery of these compounds was satisfactory, * "Wa& Polyamide B-IO" contains IO O/i anhydrous calcium sulfate as a binder (Wakb Pure Chemical fndustrics, Ltd., Nihonbashi-honcho, Chu&ku, Tokyo, Japan). J. C?~romatog.. 43 (1969) 473-479 * In the case of benzoic acicl, the absorbamy was measured at 240 mp, as benzoic acid has no absorption maximum in H,O-AcOH-MeOH (5.5 :o.s: 4).
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The quantitative analysis of benzoic and sorbic acid, methyl, ethyl and propyl esters of p-hydroxybenzoic acid and saccharin in foodstuffs is described. These compounds are quantitatively extracted with disposable clean-up columns p&ked with Extrelut@ and simultaneously determined by high-performanc
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