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Chloro­(nitrato)[1,4,7-tris(4-vinyl)­benzyl-1,4,7-tri­aza­cyclo­nonane]copper(II)

✍ Scribed by Deschamps, Jeffrey R. ;Hartshorn, Christopher M. ;Singh, Alok ;Chang, Eddie L.

Publisher
International Union of Crystallography
Year
2002
Tongue
English
Weight
199 KB
Volume
58
Category
Article
ISSN
1600-5368

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The X-ray crystal structure of the title compound, C 27 H 33 N 3 O 6 S 3 , a key intermediate in the synthesis of 1,4,7triazacyclononane and its functionalized derivatives, is presented. Two of the p-tosyl groups are coplanar with the macrocyclic ring, with the third pointing away from it.

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The title ruthenium±carbonyl complex, [Ru(C 12 H 20 N 4 )-(C 18 H 15 P)(CO)]Cl 2 Á1.5CH 2 Cl 2 , crystallizes in the triclinic space group P1 as a monomeric complex.

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✍ Fiedler, Dorothea ;Miljanić, Ognjen S. ;Welch, Eric J. 📂 Article 📅 2002 🏛 International Union of Crystallography 🌐 English ⚖ 237 KB

In the title compound, [VOCl 2 (C 9 H 21 N 3 )], the V atom is at the center of a distorted octahedral coordination sphere and is coordinated by the three N atoms of the N,N H ,N HH -trimethyl-1,4,7-triazacyclononane (Me 3 tacn) ligand, and by two chlorides and an oxo ligand.