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Chlorination of 4-methyl-8-methoxy-2,3-dihydro-1H,1,5-benzodiazepin-2-one

✍ Scribed by I. A. Abronin; L. G. Gorb; V. G. Dryuk; V. I. Sheremet; Z. F. Solomko; M. M. Kremlev

Book ID: 112348497
Publisher: Springer US
Year: 1981
Tongue: English
Weight: 227 KB
Volume: 17
Category: Article
ISSN: 0009-3122
DOI: 10.1007/bf00505607

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## Abstract Two benzodiazepines, Diazepam and Flunitrazepam, labeled with carbon‐14 in position 5 of the diazepine ring have been synthesized. Use of a condensation between iminochlorides and ^14^C‐benzonitriles, followed by exhaustive methylation of the resulting quinazolines and hydrolyses is des