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Chloramphenicol 1 (Chloromycetin). VII. Synthesis through p -Nitroacetophenone

✍ Scribed by Long, Loren M.; Troutman, H. D.

Book ID
118275375
Publisher
American Chemical Society
Year
1949
Tongue
English
Weight
364 KB
Volume
71
Category
Article
ISSN
0002-7863

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## Abstract A convenient synthesis of chloramphenicol labelled with carbon‐14 in the dichloroacetyl group at the 1 position is described. It was prepared as part of a 4‐step sequence from [1**‐**^14^C] glycine and the product was purified by preparative HPLC. A radiochemical yield of 47% was obtain