Chiral discrimination and solid-state carbon-13 NMR. Application to tri-o-thymotide clathrates
β Scribed by Ripmeester, J. A.; Burlinson, N. E.
- Book ID
- 120531377
- Publisher
- American Chemical Society
- Year
- 1985
- Tongue
- English
- Weight
- 249 KB
- Volume
- 107
- Category
- Article
- ISSN
- 0002-7863
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π SIMILAR VOLUMES
Recewcd 14 May 1980 t3C IVhfR spectra, obtamed for a number of clathrates, hydrogen-bonded complexes and polymorphic forms of hydroquinone, proved to be umquely related to the crystal structures. pquinols can easily be dlstingulshed from o-and yqumols, and hydroqumone in stolciuometric complcucs. St
13C NMR spectra of para-substituted methoxybenzenes and phenols were recorded in the solid state to gain an insight into the manner and origin of substantial peak splittings in the ortho (up to 9.2 ppm) and mefa (up to 2.5 ppm) carbon signals. It was difficult to account for these peak splittings on