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Chemoenzymatic Synthesis of O-Mannosylpeptides in Solution and on Solid Phase

✍ Scribed by Laurent, Nicolas; Both, Peter; Fontana, Carolina; Voglmeir, Josef; Weissenborn, Martin J.; Haddoub, Rose; Grassi, Paola; Haslam, Stuart M.; Šardzík, Robert; Green, Anthony P.

Book ID
111879568
Publisher
American Chemical Society
Year
2012
Tongue
English
Weight
808 KB
Volume
134
Category
Article
ISSN
0002-7863

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✍ JoséW. Nieuwenhuijzen; Paolo G.M. Conti; Harry C.J. Ottenheijm; Joannes T.M. Lin 📂 Article 📅 1998 🏛 Elsevier Science 🌐 French ⚖ 222 KB

An efficient parallel synthesis of ureas based on amino acids is described, both in solution and on solid phase, l,l'-Carbonylbisbenzotriazole 2 is used as the coupling reagent. The ureas 5 and 10 were obtained in high yield (80-100%) and purity (71-97%).