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Chemistry of acetals Communication 17. Study of the hydrolysis of diacetals of various types by gas-liquid chromatography

✍ Scribed by L. A. Yanovskaya; R. N. Stepanova

Book ID
112420111
Publisher
Springer
Year
1965
Tongue
English
Weight
479 KB
Volume
14
Category
Article
ISSN
1573-9171

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## Abstract ^17^O‐enriched acetic acid (2.5% in ^17^O) was synthesized by hydrolysis of acetic anhydride with ^17^O‐enriched water. The reaction was monitored by ^17^O and ^1^H NMR spectroscopy. Acetic anhydride, ^17^O‐enriched in both the ether and the carbonyl oxygens, was observed as an intermed