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Chemistry in Environmentally Benign Media. 7. 1 Chelating Hydroxymethyl-Functionalized Bisphosphines as Building Blocks to Water-Soluble and in-Vitro -Stable Gold(I) Complexes. Synthesis, Characterization, and X-ray Crystal Structures of [Au{(HOH 2 C) 2 PC 6 H 4 P(CH 2 OH) 2 } 2 ]Cl and [Au 2 {(HOH 2 C) 2 PCH 2 CH 2 P(CH 2 OH) 2 } 2 ]Cl 2

✍ Scribed by Berning, Douglas E.; Katti, Kattesh V.; Barnes, Charles L.; Volkert, Wynn A.; Ketring, Alan R.

Book ID: 126294285
Publisher: American Chemical Society
Year: 1997
Tongue: English
Weight: 204 KB
Volume: 36
Category: Article
ISSN: 0020-1669
DOI: 10.1021/ic961396b

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The reactions of water-soluble phosphanes P(CH,OH), (1) and Ph2PCH20H (2) with NaAuC14 in aqueous or alcoholic media, produced the water/alcoholic-soluble Au' complexes [Au(P(CH,OH),),]+ (3) and [Au(Ph2PCH20H):J+ (4) in near quantitative yields. The X-ray structures of 3 and 4, reported in this pape