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ChemInform Abstract: β-Thiopeptides: Synthesis, NMR Solution Structure, CD Spectra, and Photochemistry.

✍ Scribed by Thierry Sifferlen; Magnus Rueping; Karl Gademann; Bernhard Jaun; Dieter Seebach

Publisher
John Wiley and Sons
Year
2010
Weight
27 KB
Volume
31
Category
Article
ISSN
0931-7597

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β-Thiopeptides: Synthesis, NMR Solution
β-Thiopeptides: Synthesis, NMR Solution Structure, CD Spectra, and Photochemistry
✍ Thierry Sifferlen; Magnus Rueping; Karl Gademann; Bernhard Jaun; Dieter Seebach 📂 Article 📅 1999 🏛 John Wiley and Sons 🌐 German ⚖ 361 KB

To test the effect of NHÀCS groups (Scheme 1) on the stability of b-peptide secondary structures, we have synthesized three b-thiohexapeptide analogues of H-(b-HVal-b-HAla-b-HLeu) 2 -OH (1) with one, two, and three CS groups in the N-terminal positions (cf. 2 ± 4 and model in Fig. ). The first CS gr