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ChemInform Abstract: Titanocene-Catalyzed Reduction of Lactones to Lactols.

✍ Scribed by X. VERDAGUER; M. C. HANSEN; S. C. BERK; S. L. BUCHWALD

Publisher: John Wiley and Sons
Year: 2010
Weight: 34 KB
Volume: 29
Category: Article
ISSN: 0931-7597
DOI: 10.1002/chin.199828134

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## Abstract Electrocatalytic opening of styrene oxides (I) furnishing the corresponding primary alcohols (II) is accomplished using electrochemically reduced titanocene dichloride as catalyst, TmsCl as reagent for Ti‐O bond cleavage and 1,4‐cyclohexadiene as H‐atom donor to prevent side reactions.