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ChemInform Abstract: Synthesis of Thieno(2′,3′(3′,4′ or 3′,2′):5,6)azepino(2,1-a) isoindolediones from N-Thienyl-2(3)-ylmethylphthalimides.

✍ Scribed by P. PIGEON; B. DECROIX

Book ID
112035374
Publisher
John Wiley and Sons
Year
2010
Weight
31 KB
Volume
27
Category
Article
ISSN
0931-7597

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Synthesis and reduction of thieno[2′,3′(
Synthesis and reduction of thieno[2′,3′(3′,2′ or 3′,4′):5,6]-azocino[2,1-a]isoindole-7, 13-diones
✍ Mohamed Othman; Pascal Pigeon; Bernard Decroix 📂 Article 📅 1998 🏛 Journal of Heterocyclic Chemistry 🌐 English ⚖ 353 KB

## Abstract A synthesis of the thieno[2′,3′(3′,2′ or 3′,4′):5,6]azocino[2,1‐__a__]isoindole‐7,13‐diones 6a‐c was developed from __N__‐thienylethylphthalimides 3a‐c using a Wittig reaction followed by a Friedel‐Crafts cyclization of acetic acid derivatives 5a‐c. Reduction of ketones 6a‐c into alcoho