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ChemInform Abstract: Synthesis of Specifically Labeled Ganglioside [1c-13C]-GM3.

โœ Scribed by L. F. TIETZE; D. GRETZKE


Publisher
John Wiley and Sons
Year
2010
Weight
25 KB
Volume
29
Category
Article
ISSN
0931-7597

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Synthesis of Specifically Labelled Gangl
โœ Lutz F. Tietze; Dirk Gretzke ๐Ÿ“‚ Article ๐Ÿ“… 1998 ๐Ÿ› John Wiley and Sons ๐ŸŒ English โš– 324 KB ๐Ÿ‘ 1 views

Glycosidation of the lactose derivative 4 with [1-13 C]-sialyl sialic acid gave the trisaccharide 5 which was transformed into [1c-13 C]-GM 3 ([1c-13 C]-1). xanthate 3, prepared from enzymatically obtained [1-13 C]-FULL PAPER Scheme 2 Reagents and conditions: (a) PST, AgOTf, CH 3 CN/CH 2 Cl 2 , ฯช70ยฐ