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ChemInform Abstract: Synthesis of Phosphane Oxides and Phosphonates by Cerium-Mediated Addition of Organolithium Compounds to Chloro-Phosphorus Compounds.

✍ Scribed by Renato Dalpozzo; Antonio De Nino; Daniela Miele; Antonio Tagarelli; Giuseppe Bartoli

Publisher: John Wiley and Sons
Year: 2010
Weight: 34 KB
Volume: 30
Category: Article
ISSN: 0931-7597
DOI: 10.1002/chin.199951168

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The addition of organocerium reagents 2a-g to phosphinoyl benzyl group bound to the carbonyl moiety should be metallated. The latter reaction is the first reported synthesis chloride 1a or chlorophosphates 1b leads to the synthesis of phosphane oxides 3aa-ag and phosphonates 3bb, be in good of β-oxo

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