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ChemInform Abstract: Synthesis of Nα-Benzyloxycarbonyl-L-histidine Hydrazide: An Undesired Side-Product.
✍ Scribed by E. MASIUKIEWICZ; B. RZESZOTARSKA
- Publisher
- John Wiley and Sons
- Year
- 2010
- Weight
- 29 KB
- Volume
- 28
- Category
- Article
- ISSN
- 0931-7597
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✦ Synopsis
Synthesis of Nα-Benzyloxycarbonyl-L-histidine Hydrazide: An Undesired Side-Product. -An undisired side-product (II) is formed during the crystallization of Z-His-NH-NH2 (I). It is recommended to avoid crystallization of (I) from water and only wash the crude product with ethanol unstead.
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