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ChemInform Abstract: Synthesis of a Fluorinated Analogue of 1-Aminocyclopropane Carboxylic Acid.

✍ Scribed by M. J. SLOAN; K. L. KIRK

Publisher
John Wiley and Sons
Year
2010
Weight
29 KB
Volume
28
Category
Article
ISSN
0931-7597

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✦ Synopsis

Synthesis of a Fluorinated Analogue of 1-Aminocyclopropane Carboxylic Acid.

-In continuation of designing analogues of biologically important molecules a convenient synthesis of the 2-fluoro derivative (VII) of 1-aminocyclopropane-1-carboxylic acid is reported. Thus, cyclopropanation of the acrylate (I) followed by Curtius rearrangement, oxidative arene cleavage and deprotection provides a diastereomeric mixture of (VIII), separable by ion-exchange chromatography. -(SLOAN, M.

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