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ChemInform Abstract: Synthesis of 3- and 5-endo-(6-Chloro-3-pyridoxy)-methyl-2-azabicyclo[2.2.0]hexane and 3-endo-(6-Chloro-3-pyridoxy)-methyl-2-azabicyclo[2.2.0]hex-5-ene. ABT-594 Analogues.

✍ Scribed by Grant R. Krow; Jing Yuan; Yuhong Fang; Michael D. Meyer; David J. Anderson; Jeffrey E. Campbell; Patrick J. Carroll

Publisher: John Wiley and Sons
Year: 2001
Weight: 32 KB
Volume: 32
Category: Article
ISSN: 0931-7597
DOI: 10.1002/chin.200113117

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## Novel Conversion of Perfluoro(2,6-dimethyl-1-azacyclohexene) to 3,3,4,4,5-Pentafluoro-2,6-diphenyl-2,6-bis (trifluoromethyl)-1azabicyclo[3.1.0]hexane. -Treatment of perfluoro-azacyclohexene (I) with 2 equiv. of phenyllithium (V) in a cyclohexane/Et 2 O mixture provides access to azabicyclohex