ChemInform Abstract: Synthesis of 1,3-Dimethyl-8-(1,2,3,4-tetrahydroxybutyl)- and 1,3- Dimethyl-8-(1,2,3,4,5-pentahydroxypentyl)-7H-purine-2,6(1H,3H)-diones
β Scribed by A. RYBAR; J. ALFOELDI; M. FEDORONKO; J. KOZAK
- Book ID
- 112037005
- Publisher
- John Wiley and Sons
- Year
- 2010
- Weight
- 29 KB
- Volume
- 27
- Category
- Article
- ISSN
- 0931-7597
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## Facile Synthesis of 6-Aryl-1,3-dimethyl-5H-pyrimido[4,5b][1,4]diazepine-2,4(1H,3H)-diones. -A new approach to the regioselective synthesis of the title compounds (IV) starting from readily accessible 6-amino-5-benzylideneaminopyrimidines (I) is described. Condensation of compound (I) with diet
Single-crystal X-ray study T = 298 K Mean (C-C) = 0.005 A R factor = 0.063 wR factor = 0.167 Data-to-parameter ratio = 12.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.