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ChemInform Abstract: Synthesis and Structure of Acetyl-Substituted Oxocyclohexanecarboxylates.

✍ Scribed by V. E. Subbotin; V. V. Sorokin; A. G. Golikov; A. P. Kriven'ko

Publisher: John Wiley and Sons
Year: 2010
Weight: 19 KB
Volume: 41
Category: Article
ISSN: 0931-7597
DOI: 10.1002/chin.201041080

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are synthesized by direct reaction between the elements in a carbon-coated silica-tube (vacuum, 1000 • C, 48 h) followed by annealing at 700 • C for 4 days. X-ray powder diffraction data confirm the space group Im3 for filled skutterudites. The CeyFe 4-x NixSb 12 compounds exhibit semiconducting beh